A convenient synthesis and crystal structure of disubstituted 1,2,3-triazoles having ether functionality

Luxmi, Raj; Kaushik, C. P.; Kumar, Devinder; Kumar, Krishan; Pahwa, Ashima; Sangwan, Jyoti; Chahal, Manisha

doi:10.6084/m9.figshare.9976454.v1

lsyc_a_1672744_sm1481.docx (4.22 MB)

A convenient synthesis and crystal structure of disubstituted 1,2,3-triazoles having ether functionality

journal contribution

posted on 2019-10-14, 11:36 authored by Raj Luxmi, C. P. Kaushik, Devinder Kumar, Krishan Kumar, Ashima Pahwa, Jyoti Sangwan, Manisha Chahal

A series of 27 ether-linked 1,4-disubstituted 1,2,3-triazoles (8a–8z₁) has been synthesized by 1,3 dipolar cycloaddition of 1-substituted-4-(prop-2-yn-1-yloxy)benzene (3a–3c) and aromatic azides (5a–5c, 7a–7f). The synthesized compounds were explicated by FTIR, ¹H NMR, ¹³C NMR and HRMS techniques. The structures of synthesized triazoles 8c (CCDC 1840219) and 8f (CCDC 1840220) were also confirmed by X-ray crystallography.